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KMID : 0362219880150010117
Journal of The Korean Research Society for Dental Materials
1988 Volume.15 No. 1 p.117 ~ p.126
COMPOSITIONAL AND MICROSTRUCTURAL ANALYSIS OF SOME DENTAL AMALGAM ALLOYS USING EPMA AND X-RAY DIFFRACTION METHOD



Abstract
This research was to analyze the compositions and phases of several kinds of amalgam alloy, which were DM, HA, HV, HA 21 and OP II. The back-scattered electron images of above alloys were observed, and their compositions were analyzed by electron probe microanalyzer. The secondary electron images and back-scattered electron images of all hardened amalgams were observed and X-ray diffractometer was used to analyze the crystal phases in hardened amalgams.
The following results were obtained;
1. DM and HA were low copper amalgam alloys, and HV was unicompositional high copper amalgam alloy which was composed of Ag-Sn-Cu lathe-cut particles. HA 21 and OP II were admixed high copper amalgam alloys.
2. Cu was distributed homogeneously in spherical particle, but e phases (Cu-Sn compound) were irregularly dispersed in lathe-cut particles.
3 Hardened HV and OP II amalgams showed 71 & rh phases and 72 phases. On the other hand hardened HA 21 amalgam showed yr & n¢¥ phases, but no 72 phases.
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